SERVICES

customer contract and analytical services

Multidisciplinary expertise and research insights our clients need to develop, demonstrate and commercialize new or existing products and processes 

Our state-of-art equipment and facility and world class expertise provide lab scale R&D, scale up demonstration, data validation, data analysis and analytical needs for various chemistries at different temperature and pressure ranges to meet your product synthesis needs and/or shape a project in the areas of renewable and upcycled materials, bio-products, biomass analysis, clean energy, environmental sciences, separations, and others. We apply our capabilities that intersect with the needs of our clients, academia, commercial entities in the following practice areas of chemistry: 

  • Coupling chemistry 
    • Aldol condensation
    • Diels-Alder reaction
    • Alkylation
  • Hydrogenation 
  • Hydrodeoxygenation
  • Esterification
  • Polymerization 
  • Oligomerization
  • Depolymerization 
  • Other heterogeneous and homogeneous chemistries
  • Coupling chemistry 
    • Aldol condensation
    • Diels-Alder reaction
    • Alkylation
  • Hydrogenation 
  • Hydrodeoxygenation
  • Esterification
  • Polymerization 
  • Oligomerization
  • Depolymerization 
  • Other heterogeneous and homogeneous chemistries

We are committed to the highest standards of scientific integrity, impartiality, and objectivity.

Our Services

Process Development

Process Demonstration

Analytic Services

Process Simulation

Process Development

Process development is the key step to achieving commercial success of any technology. Many promising technologies fail because of lack of robust process knowledge at small scale. We have low pressure glass reactors, high-pressure (up to 5000 psi) and high temperature (up to 500 °C) batch and fixed bed flow reactors to meet customer’s proof-of-concept process development needs. Our expert engineers, chemists, technicians, and quality control experts work hand-on-hand to generate critical process data that ensures efficient scale-up, cost effectiveness, and process safety enabling successful translation of the project to the next step.

Process Demonstration

The next step after process development is the process demonstration prior to moving the process to pilot and commercial scale manufacturing. This is a critical step to validate  the process conditions at a reasonably larger scale, assess the process risk and mitigate risks. We have different sized batch and fixed bed flow reactors at different pressure (up to 5000 psi) and temperature (up to 500 °C) ratings to meet customers’ process demonstration needs. Our expert engineers, and chemists critically assess the process demonstration and any inherent process risks to develop solutions for customers. Our existing reactors, material of construction (MOC), dimension and operating ranges for various reactions are given below. It is continuously being updated to meet our clients’ needs. 

Reactors

Dimension/MOC

Operating range

5L mechanical stirred Parr Capacity – 5 liter

Internal Diameter: 15 cm 

Height: 31 cm

MOC: SS316

Max Pressure: 150 bar

Max Temperature : 300 °C

250 ml mechanical stirred reactor. Capacity – 250 ml

Internal Diameter: 5.7 cm 

Height: 10.8 cm

MOC: SS316

Max Pressure: 220 bar

Max Temperature: 350 °C

2L mechanical stirred Parr. Capacity – 1.9 liter

Internal Diameter: 10.1 cm 

Height: 26.6 cm

MOC: SS T316

Max Pressure: 340 bar

Max Temperature: 500 °C

OH/FH-FBR-HP-1

OH: Oil Heated

FH: Furnace Heated

FBR: Fixed bed reactor

Tube OD: 1”

Shell OD: 2” (OH)

Length: 20” max (OH)

Length: 18” (FH)

Pressure: 68 bar

Oil Heated T: 350 °C

Furnace Heated T: 1250 °C

OH/FH-FBR-HP-2

OH: Oil Heated

FH: Furnace Heated

FBR: Fixed bed reactor

Tube OD: 3/8”

Shell OD: 1” (OH)

Length: 36” (OH)

Length: 18” (FH)

Pressure – 50 bar

Oil Heated T: 350 °C

Furnace Heated T: 1250 °C

HT-FBR-LP-3

HT: Heat Tape

Tube OD: 1/5”

Length: 24”

Pressure: Ambient

Max Temperature: 500 °C

10L jacketed glass reactor with thermal liquid circulator

Capacity – 10L

MOC: Borosilicate 

Pressure: Ambient

Max Temperature: 300 °C

    1. The fixed bed reactor systems can be used for gas, liquid, and multiphase heterogeneous reactions.
    2. High pressure gas and liquid mass flow controllers, multipoint thermocouples, and data acquisition systems are available.
    3. Low pressure peristaltic pump is also available to deliver liquid reactants under ambient conditions.
    4. Fixed bed reactors are process automated. 
    5. The reactor lengths can be adjusted according to the needs.

Analytic Services

An accurate and precise characterization of products and impurities including trace impurities ensure development and delivery of acceptable quality products for desired applications. An early assessment of the products’ composition helps to optimize the process to deliver products with accepted quality. We offer a host of state-of-the-art analytical capabilities such as HPLC, GPC, GC, GCMS, viscometry (ASTM D4603), -OH number (ASTM D4274-99), carboxyl number (ASTM 4662-08) to meet clients’ analytical needs as their projects move along from process development to demonstration stages. Our expert analytical team analyzes each clients’ sample with utmost care to deliver custom reports to as-generated analytical data.

Process Simulation

Process simulation before constructing a pilot plant is vital for several reasons. It allows engineers to virtually test and optimize the production process, predicting how different variables and conditions will affect the outcomes. This minimizes risks, reduces costs, and ensures efficient resource utilization during the actual plant setup. Simulation helps identify potential bottlenecks, hazards, or inefficiencies that could arise, aiding in making informed design decisions. It also facilitates the evaluation of various scenarios, aiding in process improvement and decision-making. Our expert process engineers will use advanced process simulation tools to develop detailed models thereby enhancing the likelihood of a successful and cost-effective pilot plant implementation and subsequent full-scale production.